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HRID2040912

反应详情

EQUATION

反应方程式

HRID 2040912 的结构方程式

REACTANTS

反应物

2
结构：O=C(N1CCCC1)N1CCC2(CC(C#Cc3cccc(Cl)c3)=NO2)C1
HCID57493783

未命名化合物

结构：CC(C)(C)OC(=O)N1CCC2(CC(C#Cc3cccc(Cl)c3)=NO2)C1
HCID57493821

未命名化合物

PRODUCTS

生成物

1
结构：O=C(N1CCCC1)N1CCC2(CC1)CC(C#Cc1cccc(Cl)c1)=NO2
HCID56644864

未命名化合物

PROCEDURE

实验过程

The title compound was synthesized following the method herein described for the compound of Example 106 but replacing Compound 22d for Compound 27c. After the usual work-up procedure the crude was purified by means of automated flash chromatography (Isolera®TM-Biotage; gradient Petroleum Ether-EtOAc from 7:3 to 3:7) giving 52 mg of the title compound giving pale yellow solid. Yield: 72.6%.

WORKUP

后处理

  1. customThe title compound was synthesized
  2. customAfter the usual work-up procedure the crude was purified by means of automated flash chromatography (Isolera®TM-Biotage; gradient Petroleum Ether-EtOAc from 7:3 to 3:7)