HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → N-phenyl-2-Dibenzofuranamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | 2-Iododibenzofuran | HCID 223327 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | N-phenyl-2-Dibenzofuranamine | HCID 67204676 | — |
Reaction Steps
The Rf values of the objective substance, 2-iododibenzofuran, and aniline were respectively 0.28, 0.59, and 0.07, which were found by silica gel thin layer chromatography (TLC) (with a developing solvent of ethyl acetate and hexane in a ratio of 1:10).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580980B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-4184c7be028a4bc1bb941d5e1b8ce571 |
| Source note | uspto-grants-2013_11 |