HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentanal → 2-Methylbutanal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentanal | HCID 8063 | — |
| Reactant | 2-Propylhept-2-enal | HCID 118745 | — |
| Product | 2-Methylbutanal | HCID 7284 | — |
| Product | Pentanal | HCID 8063 | — |
| Product | 2-Propyl-4-methylhexenal | HCID 3018738 | — |
Reaction Steps
This example describes the process according to the invention for the aldol condensation of n-pentanal (n-valeraldehyde) to 2-propylheptenal (1+1 product) and the co-aldolization of n-pentanal with 2-methylbutanal to give the cross-product (1+2 product), 2-propyl-4-methylhexenal. In contrast to Example 2, the reactor used was a DN15 tube (internal diameter 17.3 mm) not of length 3 m but of length 4 m, with a total volume of 9.1 l. In this example too, about 50% of the total volume of the tubular reactor was filled with static mixers with a hydraulic diameter of 2 mm and a relative void volume of 0.80.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08581008B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-e910d27557a8461e847a849126a90a56 |
| Source note | uspto-grants-2013_11 |