HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Pentanal → 2-Methylbutanal
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Pentanal | HCID 8063 | — |
| Edukt | 2-Propylhept-2-enal | HCID 118745 | — |
| Produkt | 2-Methylbutanal | HCID 7284 | — |
| Produkt | Pentanal | HCID 8063 | — |
| Produkt | 2-Propyl-4-methylhexenal | HCID 3018738 | — |
Reaktionsschritte
This example describes the process according to the invention for the aldol condensation of n-pentanal (n-valeraldehyde) to 2-propylheptenal (1+1 product), and the co-aldolization of n-pentanal with 2-methylbutanal to give the cross-product (1+2 product), 2-propyl-4-methylhexenal. In contrast to Example 3, the total volume of the tubular reactor (DN15 tube (internal diameter 17.3 mm) with a volume of 9.1 l was filled completely with static mixers with a hydraulic diameter of 2 mm and a relative void volume of 0.80.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08581008B2 |
| Quelldatensatz | uspto-grants-2013_11 |
| ORD ID | ord-74ec4ff1f7194c43838ca97ead8e6ec6 |
| Quellennotiz | uspto-grants-2013_11 |