HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nicotinic Acid → HCID 66706738, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nicotinic Acid | HCID 938 | — |
| Reactant | HCID 57655967 | HCID 57655967 | — |
| Product | HCID 66706738 | HCID 66706738 | 185% |
Reaction Steps
Use a method similar to Example 42, using nicotinic acid (40 mg, 0.327 mmol) and 6-(2-amino-ethoxy)-7-chloro-3-(2,2,2-trifluoroacetyl)-2,3,4,5-tetrahydro-1H-benzo[d]azepine (100 mg, 0.297 mmol) to give the title compound as a solid (105 mg, 93%). MS (ES+) m/z: 346 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08580780B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-25ba17bc6f274b8baecef680f95e5f32 |
| Source note | uspto-grants-2013_11 |