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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2041407Generated: November 2, 2026

Methyl bromoacetate → HCID 66707067, compound

https://huagongshe.com/reaction/2041407

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl bromoacetateHCID 60984—
Reactant3-tert-butoxycarbonyl-7-chloro-6-dimethylaminocarbonylthio-2,3,4,5-tetrahydro-1H-benzo[d]azepineHCID 57655979—
ProductHCID 66707067HCID 66707067—

Reaction Steps

Use a method similar to the Example 347, using 3-tert-butoxycarbonyl-7-chloro-6-dimethylcarbamoylthio-2,3,4,5-tetrahydro-1H-benzo[d]azepine and methyl bromoacetate to give 3-tert-butoxycarbonyl-7-chloro-6-methoxycarbonylmethylthio-2,3,4,5-tetrahydro-1H-benzo[d]azepine.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08580780B2
Source datasetuspto-grants-2013_11
ORD IDord-2f06520cdc674a5d98d2e060f547f912
Source noteuspto-grants-2013_11