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HRID2041413

反应详情

EQUATION

反应方程式

HRID 2041413 的结构方程式

REACTANTS

反应物

2
结构：Br.BrCCc1ccccn1
HCID12913859

2-(2-Bromoethyl)pyridine--hydrogen bromide (1/1)

C7H9Br2N

结构：CN(C)C(=O)Sc1c(Cl)ccc2c1CCN(C(=O)OC(C)(C)C)CC2
HCID57655979

未命名化合物

PRODUCTS

生成物

1
结构：Cl.Clc1ccc2c(c1SCCc1ccccn1)CCNCC2
HCID66706873

未命名化合物

PROCEDURE

实验过程

Use a method similar to the Preparation 177, using 3-tert-butoxycarbonyl-7-chloro-6-dimethylcarbamoylthio-2,3,4,5-tetrahydro-1H-benzo[d]azepine and 2-(2-bromoethyl)-pyridine hydrobromide to give, after deprotection using a method similar to the General Procedure 1-4, the title compound. MS (ES+) m/z 319 (M+H)+.

WORKUP

后处理

  1. customsimilar to the Preparation 177
  2. customto give