Phenylacetylene → HCID 53247079, compound

HRID 2042144Notes

Reaction equation

HRID 2042144 reaction equation
Br[C:2]1[CH:3]=[N:4][C:5]2[N:6]([N:8]=[C:9]([C:11]([CH3:14])([CH3:13])[CH3:12])[CH:10]=2)[CH:7]=1.[C:15]1([C:21]#[CH:22])[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[C:11]([C:9]1[CH:10]=[C:5]2[N:4]=[CH:3][C:2]([C:22]#[C:21][C:15]3[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=3)=[CH:7][N:6]2[N:8]=1)([CH3:14])([CH3:13])[CH3:12]

Participants

3

Reactant 2

HCID 10821PhenylacetyleneHCID 583166976-Bromo-2-tert-butylpyrazolo[1,5-a]pyrimidine

Product 1

HCID 53247079HCID 53247079, compound

Procedure

The title compound, light yellow solid, MS: m/e=276.2 (M+H+), can be prepared in accordance with the general method of example 1 from 6-bromo-2-tert-butyl-pyrazolo[1,5-a]pyrimidine (example 9, step 1) and phenylacetylene.

Sources & evidence

ORD record
ord-cd5ece5570d84b10b92b5885bac95358
Source dataset
uspto-grants-2013_11
Patent number
US08586581B2

Reaction notes

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