Phenylacetylene → HCID 50913011, compound

HRID 2042171Notes

Reaction equation

HRID 2042171 reaction equation
[N:1]1[N:5]2[CH:6]=[C:7](OS(C(F)(F)F)(=O)=O)[CH:8]=[CH:9][C:4]2=[CH:3][CH:2]=1.[C:18]1([C:24]#[CH:25])[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>>[C:18]1([C:24]#[C:25][C:7]2[CH:8]=[CH:9][C:4]3[N:5]([N:1]=[CH:2][CH:3]=3)[CH:6]=2)[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1

Participants

3

Reactant 2

HCID 10821PhenylacetyleneHCID 58316721HCID 58316721, compound

Product 1

HCID 50913011HCID 50913011, compound

Procedure

The title compound, light yellow solid, MS: m/e=219.2 (M+H+), can be prepared in accordance with the general method of example 1 from trifluoro-methanesulfonic acid pyrazolo[1,5-a]pyridin-6-yl ester (example 33, step 2) and phenylacetylene.

Sources & evidence

ORD record
ord-bcb960b8dd234345bd1624b5c6a49fdc
Source dataset
uspto-grants-2013_11
Patent number
US08586581B2

Reaction notes

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