Phenylacetylene → HCID 53247452, compound

HRID 2042172Notes

Reaction equation

HRID 2042172 reaction equation
Br[C:2]1[CH:3]=[CH:4][C:5]2[N:6]([N:8]=[N:9][CH:10]=2)[CH:7]=1.[C:11]1([C:17]#[CH:18])[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1>>[C:11]1([C:17]#[C:18][C:2]2[CH:3]=[CH:4][C:5]3[N:6]([N:8]=[N:9][CH:10]=3)[CH:7]=2)[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1

Participants

3

Reactant 2

HCID 10821PhenylacetyleneHCID 159399556-broMo-[1,2,3]triazolo[1,5-a]pyridine

Product 1

HCID 53247452HCID 53247452, compound

Procedure

The title compound, light brown solid, MS: m/e=220.3 (M+H), can be prepared in accordance with the general method of example 1 from 6-bromo-[1,2,3]triazolo[1,5-a]pyridine (example 34, step 1) and phenylacetylene.

Sources & evidence

ORD record
ord-1af9fe3b929747b4b816d87bd51f7751
Source dataset
uspto-grants-2013_11
Patent number
US08586581B2

Reaction notes

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