2-Bromopropanedial → HCID 58316703, compound
Reaction equation
[N:1]1([C:7]2[N:8]=[C:9]([NH2:12])[NH:10][N:11]=2)[CH2:6][CH2:5][O:4][CH2:3][CH2:2]1.[Br:13][CH:14]([CH:17]=O)[CH:15]=O>>[Br:13][C:14]1[CH:15]=[N:12][C:9]2[N:10]([N:11]=[C:7]([N:1]3[CH2:2][CH2:3][O:4][CH2:5][CH2:6]3)[N:8]=2)[CH:17]=1Participants
3
Procedure
The title compound, a light yellow solid, MS: m/e=284.2/286.1 (M+H+), can be prepared in accordance with the general method of example 42, step 1 from 5-morpholin-4-yl-2H-[1,2,4]triazol-3-ylamine (CAS 51420-46-3) and 2-bromomalonaldehyde.
Sources & evidence
- ORD record
- ord-77c58061b38f49838a9792c54bd3b1dd
- Source dataset
- uspto-grants-2013_11
- Patent number
- US08586581B2
Reaction notes
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