HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanesulfonyl chloride → HCID 178477731, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanesulfonyl chloride | HCID 11667 | — |
| Reactant | HCID 178478592 | HCID 178478592 | — |
| Product | HCID 178477731 | HCID 178477731 | — |
Reaction Steps
The title compound, light brown foam (77 mg, 54%), MS (ISP) m/z=421.2 [(M+H)+], was prepared in analogy to example 14 starting from trans-4-[2-(4-furo[3,2-c]pyridin-4-yl-piperazin-1-yl)-ethyl]-cyclohexylamine trihydrochloride (intermediate A) (150 mg, 0.34 mmol) and ethanesulfonyl chloride (88 mg, 0.68 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586579B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-1f77449cc2d944c6a0c0c68f465027f5 |
| Source note | uspto-grants-2013_11 |