Acetic Acid → HCID 178474981, compound

Participants

Reaction Steps

The title compound, off-white solid (47 mg, 81%), MS (ISP) m/z=387.4 [(M+H)+], mp 196.5° C., was prepared in accordance with the general method of example 32 from trans-4-{2-[4-(7-methyl-2,3-dihydro-furo[3,2-c]pyridin-4-yl)-piperazin-1-yl]-ethyl}-cyclohexylamine trihydrochloride (intermediate G) (68.1 mg, 0.15 mmol) and acetic acid.

Provenance & Evidence