huagongshe.com
HRID2042502

反应详情

EQUATION

反应方程式

HRID 2042502 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)CCC(OC)OC
HCID350846

Methyl 4,4-dimethoxybutyrate

C7H14O4

结构：Cl.Cl.Cl.N[C@H]1CC[C@H](CCN2CCN(c3nccc4c3CCO4)CC2)CC1
HCID178478589

未命名化合物

2 次

PRODUCTS

生成物

1
结构：COC(CCC(=O)N[C@H]1CC[C@H](CCN2CCN(c3nccc4c3CCO4)CC2)CC1)OC
HCID178495091

未命名化合物

PROCEDURE

实验过程

The title compound, white solid (114 mg, 99%), MS (ISP) m/z=461.5 [(M+H)+], mp 205.5° C., was prepared in accordance with the general method of example 2 from trans-{2-[4-(2,3-dihydrofuro[3,2-c]pyridin-4-yl)-piperazin-1-yl]-ethyl}-cyclohexanamine trihydrochloride (intermediate C) (110 mg, 0.25 mmol) and methyl 4,4-dimethoxy-butanoate.