1,3-Benzodioxole-5-carboxylic acid → HCID 178523693, compound

Participants

Reaction Steps

The title compound, white solid (107 mg, 89%), MS (ISP) m/z=479.3 [(M+H)+], mp 243.5° C., was prepared in accordance with the general method of example 32 from trans-4-{2-[4-(2,3-dihydrofuro[3,2-c]pyridin-4-yl)-piperazin-1-yl]-ethyl}-cyclohexanamine trihydrochloride (intermediate C) (110 mg, 0.25 mmol) and benzo[1,3]dioxole-5-carboxylic acid.

Provenance & Evidence