HuagongsheHuagongshe Chemistry Print Report · For research reference only
ETHYL 2-(1-HYDROXYCYCLOBUTYL)ACETATE → HCID 178520405, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | ETHYL 2-(1-HYDROXYCYCLOBUTYL)ACETATE | HCID 58134840 | — |
| Reactant | HCID 178478589 | HCID 178478589 | — |
| Product | HCID 178520405 | HCID 178520405 | — |
Reaction Steps
The title compound, white solid (58 mg, 52%), MS (ISP) m/z=443.5 [(M+H)+], mp 155° C., was prepared in accordance with the general method of example 2 from trans-4-{2-[4-(2,3-dihydrofuro[3,2-c]pyridin-4-yl)-piperazin-1-yl]-ethyl}-cyclohexanamine trihydrochloride (intermediate C) (110 mg, 0.25 mmol) and ethyl 2-(1-hydroxy-cyclobutyl)-acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586579B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-543333e64eda423ba82d9226df4cde26 |
| Source note | uspto-grants-2013_11 |