HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 57399329, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 59651964 | HCID 59651964 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 57399329 | HCID 57399329 | — |
Reaction Steps
The product from step 4 (0.75 g, 2.1 mmol) and hydrazine hydrate (2.0 mL) in acetonitrile (25 mL) were heated to reflux for 24 h. The reaction was cooled, concentrated and the product recrystallized using Et2O-hexanes to give 600 mg (71%); Mp 118-121; MS m/z 344 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586588B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-e02edbe3bac3479d814468325305f766 |
| Source note | uspto-grants-2013_11 |