HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Thiopheneacetyl chloride → HCID 67251903, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Thiopheneacetyl chloride | HCID 162362 | — |
| Reactant | (S)-N-(8-methoxytetralin-2-yl)-N-propylamine | HCID 12741415 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 67251903 | HCID 67251903 | — |
Reaction Steps
Synthesis worked according to the preparation of A4-1 when using 310 mg (1.4 mmol) enantiomerical pure (S)—N-(8-methoxytetralin-2-yl)-N-propylamine ((R)-A2-1: R═OMe) and 0.35 mL (2.8 mmol) 2-thienyl acetic acid chloride. Flash chromatography was done with hexane/ethyl acetate 20/1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586603B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-6946bf702dc54362ad038d747612fa46 |
| Source note | uspto-grants-2013_11 |