HuagongsheHuagongshe Chemistry Print Report · For research reference only
8-methoxy-N-propyl-1,2,3,4-tetrahydronaphthalen-2-amine → HCID 178457758, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 8-methoxy-N-propyl-1,2,3,4-tetrahydronaphthalen-2-amine | HCID 12741417 | — |
| Reactant | Cyclopenta-1,3-diene;2-cyclopenta-2,4-dien-1-ylacetic acid;iron(2+) | HCID 15768501 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 178457758 | HCID 178457758 | — |
Reaction Steps
Synthesis worked according to the preparation of A4-4 when using 360 mg (1.6 mmol) N-(8-methoxytetralin-2-yl)-N-propylamine (A2-1: R═OMe) and 240 mg (0.99 mmol) ferrocenylacetic acid (A3-7: W═OH, Cy=ferrocenyl). Flash chromatography of the residue on silica gel with a mixture of hexane/ethyl acetate 10/1 gave the crude product N-(8-methoxytetralin-2-yl)-N-propyl-2-ferrocenylacetamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586603B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-2de50ea394804b8ebac31ed3b5e78638 |
| Source note | uspto-grants-2013_11 |