HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Thiocarbonyldi-2(1H)-pyridone → N-(2,4-Dichloro-3-isothiocyanato-benzyl)-1-trifluoromethyl-cyclopropane carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Thiocarbonyldi-2(1H)-pyridone | HCID 853162 | — |
| Reactant | N-(2,4-Dichloro-3-amino-benzyl)-1-trifluoromethyl-cyclopropane carboxamide | HCID 56839976 | — |
| Product | N-(2,4-Dichloro-3-isothiocyanato-benzyl)-1-trifluoromethyl-cyclopropane carboxamide | HCID 56840197 | — |
Reaction Steps
The title compound is prepared from N-(2,4-dichloro-3-amino-benzyl)-1-trifluoromethyl-cyclopropane carboxamide (150 mg, 0.45 mmol) and 1,1′-thiocarbonyldi-2-pyridone (89 mg, 0.38 mmol) in analogy to example Af.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586604B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-a1f36131017c4b5bb9891572c7ddb579 |
| Source note | uspto-grants-2013_11 |