HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl chloroformate → HCID 86680899, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl chloroformate | HCID 61140 | — |
| Reactant | HCID 51346777 | HCID 51346777 | — |
| Solvent | 2,6-Lutidine | HCID 7937 | — |
| Product | HCID 86680899 | HCID 86680899 | 50.5% |
Reaction Steps
To a solution of 48 (200 mg, 0.44 mmol) in 2,6-lutidine (2.0 ml) was added butyl chloroformate (73 μl, 0.57 mmol) at 0° C. and stirred at room temperature for 2 h. The crude product was purified by prep HPLC (C18) to provide the titled compound (123 mg, 50%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586550B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-7c0aeb1ddb35417f815f65ee12ae75bb |
| Source note | uspto-grants-2013_11 |