HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl disulfide → HCID 178454949, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl disulfide | HCID 12386 | — |
| Reactant | HCID 178503312 | HCID 178503312 | — |
| Reactant | HCID 178506560 | HCID 178506560 | — |
| Solvent | Diethylether ethylacetate | HCID 21584169 | — |
| Product | HCID 178454949 | HCID 178454949 | 18.4% |
Reaction Steps
Compound 21F was prepared following the procedure as described for the synthesis of compound 21A (see Scheme 3) using 1-butyldisulfanyl-butane as the disulfide and 3-(4-iodo-1H-pyrazol-3-yl)-pyridine (compound 20B). (flash chromatography conditions ethyl acetate/diethyl ether 3/1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586606B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-d8593479671448138ab441318550fa03 |
| Source note | uspto-grants-2013_11 |