HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 53627594, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Benzotriazol-1-yloxy-tris(dimethylamino)phosphonium hexafluorophosphate | HCID 151348 | — |
| Reactant | (r)-2-(4-Fluoro-1h-indol-1-yl)propanoic acid | HCID 57425928 | — |
| Reactant | 4-(piperazin-1-yl)-N-(thiazol-2-yl)benzenesulfonamide | HCID 59466506 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 53627594 | HCID 53627594 | — |
Reaction Steps
Synthesized according to general procedure 5, method A. The reaction was set up with 0.08 mmol 4-(piperazin-1-yl)-N-(thiazol-2-yl)benzenesulfonamide, 0.08 mmol (2R)-2-(4-fluoro-indol-1-yl)-propionic acid, 0.08 mmol BOP reagent, 0.08 mmol triethylamine and 200 μL DMF. LC/MS (10%-99% CH3CN (0.035% TFA)/H2O (0.05% TFA)), m/z: M+1 obs=514.50; tR=3.03 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586589B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-65dd5a979c1041d2acea7b08917434d5 |
| Source note | uspto-grants-2013_11 |