HCID 129777790, compound → HCID 131731048, compound

Participants

Reaction Steps

BnO-GlyLys [α-CO-3,5-Ph(CO2Me)2] [ε-Glu] [α-Boc] [γ-CO2Me] (90 mg, 0.119 mmol) was dissolved in 2,2,2-trifluoroethanol (4 ml) and stirred at room temperature. Non-Degussa Pd/C (10%, 0.030 mmol, 32 mg) was added to the degassed solution and the system was stirred under hydrogen gas (1 atm) for 24 h. The catalyst was removed by filtration and the filtrate was concentrated to dryness to give HO-GlyLys [α-CO-3,5-Ph(CO2Me)2] [ε-Glu] [α-Boc] [γ-CO2Me] as an orange glass (81 mg, 102%).

Provenance & Evidence