HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromotrimethylsilane → (12-Bromododecyl)phosphonic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromotrimethylsilane | HCID 76113 | — |
| Reactant | HCID 11773557 | HCID 11773557 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | (12-Bromododecyl)phosphonic acid | HCID 45158982 | — |
Reaction Steps
The compound BDPA was synthesized in two steps. In the first step, diethyl 12-bromododecylphosphonate is prepared as specified in Example 1. In the second step, diethyl 12-bromododecylphosphonate (2.43 g; 6.32 mmol) is reacted with Me3SiBr (2.89 g; 18.93 mmol) in 50 ml of dry CH2Cl2 with stirring at room temperature for 12 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586758B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-07547860103f4341a640750966df406a |
| Source note | uspto-grants-2013_11 |