HuagongsheHuagongshe Chemistry Print Report · For research reference only
((2-Chloroethyl)sulphonyl)benzene → HCID 67134364, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | ((2-Chloroethyl)sulphonyl)benzene | HCID 13646 | — |
| Reactant | 2-Methylnicotinic acid | HCID 643373 | — |
| Product | HCID 67134364 | HCID 67134364 | 16% |
Reaction Steps
Starting from 2.1 g (15.0 mmol) of 2-methyl-nicotinic acid and 4.6 g (22.5 mmol) of (2-chloroethyl)-phenylsulfone, 0.7 g (2.4 mmol, 16%) of 2-(3-(phenylsulfonyl)propyl)-nicotinic acid was obtained according to the process described in precursor VB006.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586755B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-9bccac4b67f542e1b7d182935dfd2e51 |
| Source note | uspto-grants-2013_11 |