HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorophenylhydrazine hydrochloride → HCID 58204707, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorophenylhydrazine hydrochloride | HCID 443287 | — |
| Reactant | HCID 58204698 | HCID 58204698 | — |
| Product | HCID 58204707 | HCID 58204707 | 59% |
Reaction Steps
Following the procedure in Example 22, methyl 2-((dimethylamino)methylenecarbamoyl)-5,6-dihydrobenzo[f]imidazo[1,2-d][1,4]oxazepine-10-carboxylate was coupled with 2-chlorophenylhydrazine hydrochloride to give methyl 2-(1-(2-chlorophenyl)-1H-1,2,4-triazol-5-yl)-5,6-dihydrobenzo[f]imidazo[1,2-d][1,4]oxazepine-10-carboxylate. Yield 59%. MS (ESI+): 422.1
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586574B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-e5248296c32e4ad189c2786e0592f6a9 |
| Source note | uspto-grants-2013_11 |