HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2044261Generated: October 29, 2026
1,1-Dimethoxyethyl(dimethyl)amine → HCID 178464914, compound
https://huagongshe.com/reaction/2044261
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1,1-Dimethoxyethyl(dimethyl)amine | HCID 87835 | — |
| Reactant | 9-Bromo-5,6-dihydrobenzo[f]imidazo[1,2-d][1,4]oxazepine-2-carboxamide | HCID 58204629 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 178464914 | HCID 178464914 | — |
Reaction Steps
To a solution of 8-Bromo-4,5-dihydro-6-oxa-1,3a-diaza-benzo[e]azulene-2-carboxylic acid amide (0.280 g, 0.000909 mol) in toluene (5 mL) was added dimethylacetamide-dimethylacetal (0.405 mL, 0.00273 mol). The solution was stirred at 95° C. for 4 h. The toluene was removed in vacuo to give 8-Bromo-4,5-dihydro-6-oxa-1,3a-diaza-benzo[e]azulene-2-carboxylic acid [1-dimethylamino-eth-(E)-ylidene]-amide. MS (ESI+) 377.1/379.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08586574B2 |
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| Source dataset | uspto-grants-2013_11 |
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| ORD ID | ord-8afcc4d18d2546beac10920898eaad22 |
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| Source note | uspto-grants-2013_11 |
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