HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Isopropylhydrazine hydrochloride → HCID 58204990, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Isopropylhydrazine hydrochloride | HCID 85573 | — |
| Reactant | HCID 140563933 | HCID 140563933 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 58204990 | HCID 58204990 | — |
Reaction Steps
1-(8-Bromo-4,5-dihydro-6-oxa-1,3a-diaza-benzo[e]azulene-2-carbonyl)-2-methyl-isothiourea (27 mg, 0.068 mmol) was heated with isopropylhydrazine hydrochloride (23 mg, 0.20 mmol) in acetic acid (0.9 mL) at 100° C. overnight. The mixture was concentrated and the crude residue purified by reverse-phase HPLC to give 240. LCMS EI: 422.1
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586574B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-cf7e19556e6a4e7d848c618f0b646b92 |
| Source note | uspto-grants-2013_11 |