HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonyl chloride → HCID 68407000, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonyl chloride | HCID 7369 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-Nitro-4-(piperidin-4-ylamino)benzenesulfonamide | HCID 43345806 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 68407000 | HCID 68407000 | — |
Reaction Steps
A mixture of EXAMPLE 157B (84 mg), benzenesulfonyl chloride (46 mg), and triethylamine (101 mg) in CH2Cl2 (2 mL) was stirred for 1 hours. The product was chromatographed on silica gel with 25% ethyl acetate/hexanes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586754B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-4347e09383e3498f8c4d0ea9b11b63c7 |
| Source note | uspto-grants-2013_11 |