HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzaldehyde → HCID 178498134, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzaldehyde | HCID 541 | — |
| Reactant | Methyl 4-aminobenzoate | HCID 12082 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178498134 | HCID 178498134 | 103.1% |
Reaction Steps
A mixture of methyl 4-aminobenzoate (1.51 g, 10 mmol) and 4-nitrobenzaldehyde (1.51 g, 10 mmol) in ethanol (30 mL) was stirred overnight to give the yellow slurry. The precipitated off-white solid was collected and dried in vacuo to give (E)-methyl 4-(4-nitrobenzylideneamino)benzoate (2.93 g, 95% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08586747B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-c1deb03f1a134b3bbbe26b09e2c5a64d |
| Source note | uspto-grants-2013_11 |