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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2045739Generated: October 30, 2026

Water → HCID 4379666, compound

https://huagongshe.com/reaction/2045739

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantBenzyl ChlorideHCID 7503—
ReactantPotassium CarbonateHCID 11430—
Reactant3-BromocarbazoleHCID 252446—
SolventTetrahydrofuranHCID 8028—
ProductHCID 4379666HCID 437966691.5%

Reaction Steps

24 g of 3-bromocarbazole was dissolved in 100 ml of tetrahydrofuran. To this was added 14 g of potassium carbonate followed by 14 g of benzylchloride and allowed the reaction to stir at room temperature overnight. The reaction mixture was poured into water and the precipitated white solid was filtered, washed with methanol and dried under vacuum to obtain 30 g 9-benzyl-3-bromocarbazole (89%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08592055B2
Source datasetuspto-grants-2013_11
ORD IDord-da238b6611824c159c600bee1b80106b
Source noteuspto-grants-2013_11