HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 4379666, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3-Bromocarbazole | HCID 252446 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 4379666 | HCID 4379666 | 91.5% |
Reaction Steps
24 g of 3-bromocarbazole was dissolved in 100 ml of tetrahydrofuran. To this was added 14 g of potassium carbonate followed by 14 g of benzylchloride and allowed the reaction to stir at room temperature overnight. The reaction mixture was poured into water and the precipitated white solid was filtered, washed with methanol and dried under vacuum to obtain 30 g 9-benzyl-3-bromocarbazole (89%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592055B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-da238b6611824c159c600bee1b80106b |
| Source note | uspto-grants-2013_11 |