3,4'-Dichloropropiophenone → HCID 58295221, compound

HRID 2045825Notes

Reaction equation

[CH2:1]([NH:8][CH2:9][CH2:10][NH2:11])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Cl[CH2:13][CH2:14][C:15]([C:17]1[CH:22]=[CH:21][C:20]([Cl:23])=[CH:19][CH:18]=1)=O>>[CH2:1]([N:8]1[CH2:13][CH2:14][CH:15]([C:17]2[CH:22]=[CH:21][C:20]([Cl:23])=[CH:19][CH:18]=2)[NH:11][CH2:10][CH2:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

Reactant 2

HCID 775503,4'-Dichloropropiophenone

HCID 77801N-Benzylethylenediamine

Product 1

HCID 58295221HCID 58295221, compound

Procedure

This compound was prepared by the method of preparation 2 starting from N-benzylethylenediamine but using commercially available 3-chloro-1-(4-chlorophenyl)propan-1-one. LRMS: APCl+ m/z 300 [MH+].

Sources & evidence

ORD record: ord-7d6fac6156ef4ee7b2521d3dc16d3646
Source dataset: uspto-grants-2013_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08592403B2

Reaction notes

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