HuagongsheHuagongshe Chemistry Print Report · For research reference only
(5-Chlorobenzofuran-3-yl)methanol → 4-((5-Chlorobenzofuran-3-yl)methoxy)benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (5-Chlorobenzofuran-3-yl)methanol | HCID 3757833 | — |
| Reactant | 4-Methoxy-3-tricyclo[3.3.1.13,7]dec-1-ylbenzaldehyde | HCID 54029530 | — |
| Product | 4-((5-Chlorobenzofuran-3-yl)methoxy)benzaldehyde | HCID 87074984 | 9% |
Reaction Steps
When the product of Step A was substituted for 3-(1-admantanyl)-4-methoxy benzaldehyde in Example 32, Step B, the similar procedure afforded the title compound in 9% yield, as pale paste. 1H-NMR (CDCl3) 9.89 (s, 1H); 7.84 (d, 2H, J=8.74 Hz); 7.72 (s, 1H); 7.60 (d, 1H, J=2.07 Hz); 7.41 (d, 1H, J=8.76 Hz); 7.28 (dd, 1H, J=8.75, 2.09 Hz); 7.09 (d, 2H, J=8.73 Hz); 5.23 (s, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592399B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-c50d5680f3b146f98719655f0ab200d9 |
| Source note | uspto-grants-2013_11 |