HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-butyl N-(2-hydroxyethyl)carbamate → (rac)-2-(1-Phenoxy-ethyl)-6,7-dihydro-5H-pyrazolo[1,5-a]pyrazin-4-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-butyl N-(2-hydroxyethyl)carbamate | HCID 2733206 | — |
| Reactant | 2-(phenoxymethyl)-6,7-dihydropyrazolo[1,5-a]pyrazin-4(5H)-one | HCID 57411799 | — |
| Reactant | ethyl 1-{2-[(tert-butoxycarbonyl)amino]propyl}-3-(phenoxymethyl)-1H-pyrazole-5-carboxylate | HCID 67958408 | — |
| Reactant | HCID 178468931 | HCID 178468931 | — |
| Product | (rac)-2-(1-Phenoxy-ethyl)-6,7-dihydro-5H-pyrazolo[1,5-a]pyrazin-4-one | HCID 67974295 | — |
Reaction Steps
The compound was prepared from (rac)-5-(1-phenoxy-ethyl)-2H-pyrazole-3-carboxylic acid ethyl ester and tert-butyl n-(2-hydroxyethyl)carbamate using the methods described in the preceding examples 7 ((rac)-2-(2-tert-butoxycarbonylamino-propyl)-5-phenoxymethyl-2H-pyrazole-3-carboxylic acid ethyl ester) and 6 (2-phenoxymethyl-6,7-dihydro-5H-pyrazolo[1,5-a]pyrazin-4-one).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592422B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-3846b304d3334993be2ee6beebfbc7f8 |
| Source note | uspto-grants-2013_11 |