Dimethylamine → 6-Chloro-N,N,4-trimethyl-2-pyridinamine

HRID 2046240Notes

Reaction equation

HRID 2046240 reaction equation
[Cl:1][C:2]1[CH:7]=[C:6]([CH3:8])[CH:5]=[C:4](Cl)[N:3]=1.[CH3:10][NH:11][CH3:12].ClC1N=C(N(C)C)C=CC=1C.ClC1N=C(N(C)C)C(C)=CC=1>>[Cl:1][C:2]1[N:3]=[C:4]([N:11]([CH3:12])[CH3:10])[CH:5]=[C:6]([CH3:8])[CH:7]=1

Participants

5

Reactant 4

HCID 674DimethylamineHCID 108989972,6-Dichloro-4-methylpyridineHCID 86670205(6-Chloro-5-methyl-pyridin-2-yl)-dimethyl-amineHCID 86670206(6-Chloro-3-methyl-pyridin-2-yl)-dimethyl-amine

Product 1

HCID 589232276-Chloro-N,N,4-trimethyl-2-pyridinamine

Procedure

The compound was prepared from 2,6-dichloro-4-methylpyridine and dimethylamine using the method described in the preceding example 86 (6-chloro-5-methyl-pyridin-2-yl)-dimethyl-amine and (6-chloro-3-methyl-pyridin-2-yl)-dimethyl-amine).

Sources & evidence

ORD record
ord-bea611a23e414a35bb6c2cff43607e63
Source dataset
uspto-grants-2013_11
Patent number
US08592422B2

Reaction notes

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