HRID2046325

反应详情

EQUATION

反应方程式

HRID 2046325 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Pd—C (371 mg) was added to a solution of Compound 30 (3.7 g) in methanol (111 ml) and then, hydrogenation was carried out by stirring the mixture at atmospheric pressure and room temperature overnight. Subsequently, the catalyst was removed by filtration and the filtrate was concentrated under reduced pressure to give 2.9 g (96% yield) of the title compound.

WORKUP

后处理

  1. customSubsequently, the catalyst was removed by filtration
  2. concentrationthe filtrate was concentrated under reduced pressure