4-Methylbenzaldehyde → 4-(4-Methylphenyl)-3-buten-2-one

HRID 2046442Notes

Reaction equation

[CH3:1][C:2]1[CH:9]=[CH:8][C:5]([CH:6]=O)=[CH:4][CH:3]=1.C[O:11][C:12]1[CH:17]=CC=C[C:13]=1C=CC(=O)C>>[C:2]1([CH3:1])[CH:9]=[CH:8][C:5]([CH:6]=[CH:13][C:12](=[O:11])[CH3:17])=[CH:4][CH:3]=1

Participants

Reactant 2

HCID 77254-Methylbenzaldehyde

HCID 139181o-Anisalacetone

Product 1

HCID 1073884-(4-Methylphenyl)-3-buten-2-one

Procedure

The title compound was prepared from 4-methyl-benzaldehyde (6.0 g, 50.0 mmol), following the procedure describing the synthesis of 4-(2-methoxy-phenyl)-but-3-en-2-one (example 1/a stage 1).

Sources & evidence

ORD record: ord-89e808bce2d74c658b64d1641b486cd6
Source dataset: uspto-grants-2013_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08592430B2

Reaction notes

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