4-(4-Methylphenyl)-3-buten-2-one → 5-(4-Methylphenyl)cyclohexane-1,3-dione

HRID 2046443Notes

Reaction equation

HRID 2046443 reaction equation
[C:1]1([CH3:12])[CH:6]=[CH:5][C:4]([CH:7]=[CH:8][C:9](=[O:11])[CH3:10])=[CH:3][CH:2]=1.C[O:14][C:15]1C=CC=C[C:16]=1C1CC(=O)CC(=O)C1>>[C:1]1([CH3:12])[CH:2]=[CH:3][C:4]([CH:7]2[CH2:8][C:9](=[O:11])[CH2:10][C:15](=[O:14])[CH2:16]2)=[CH:5][CH:6]=1

Participants

3

Reactant 2

HCID 1073884-(4-Methylphenyl)-3-buten-2-oneHCID 171223135-(2-Methoxyphenyl)-1,3-cyclohexanedione

Product 1

HCID 5764925-(4-Methylphenyl)cyclohexane-1,3-dione

Procedure

The title compound was prepared from 4-p-tolyl-but-3-en-2-one stage 1 (4.8 g, 30.0 mmol), following the procedure describing the synthesis of 5-(2-methoxy-phenyl)-cyclohexane-1,3-dione (example 1/a stage 2).

Sources & evidence

ORD record
ord-d70d738a54ab483eb6ffd7a0fba5afe5
Source dataset
uspto-grants-2013_11
Patent number
US08592430B2

Reaction notes

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