o-Anisalacetone → HCID 67065312, compound

HRID 2046448Notes

Reaction equation

HRID 2046448 reaction equation
[Br:1][C:2]1[CH:9]=[C:8]([F:10])[CH:7]=[CH:6][C:3]=1[CH:4]=O.C[O:12][C:13]1[CH:18]=CC=C[C:14]=1C=CC(=O)C>>[Br:1][C:2]1[CH:9]=[C:8]([F:10])[CH:7]=[CH:6][C:3]=1[CH:4]=[CH:14][C:13](=[O:12])[CH3:18]

Participants

3

Procedure

The title compound was prepared from 2-bromo-4-fluoro-benzaldehyde (30 g, 148 mmol), following the procedure describing the synthesis of 4-(2-methoxy-phenyl)-but-3-en-2-one (example 1/a stage 1).

Sources & evidence

ORD record
ord-4987b7dd869b43d087549540855f0e33
Source dataset
uspto-grants-2013_11
Patent number
US08592430B2

Reaction notes

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