HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(4-Chlorophenyl)-2-[(dimethylamino)methylene]-1,3-cyclohexanedione → 2-Dimethylaminomethylene-5-phenyl-cyclohexane-1,3-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(4-Chlorophenyl)-2-[(dimethylamino)methylene]-1,3-cyclohexanedione | HCID 567070 | — |
| Reactant | 1,3-Cyclohexanedione, 5-phenyl- | HCID 568962 | — |
| Product | 2-Dimethylaminomethylene-5-phenyl-cyclohexane-1,3-dione | HCID 10890110 | — |
Reaction Steps
The title compound was prepared from 5-phenylcyclohexane-1,3-dione (1.0 g, 5.3 mmol), following the procedure described for the synthesis of 5-(4-chloro-phenyl)-2-dimethylaminomethylene-cyclohexane-1,3-dione (example 2/a stage 1) except that the reaction was run at ambient temperature for 30 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592430B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-0128f0eba9e84a23a2e582bf1bd4a1de |
| Source note | uspto-grants-2013_11 |