HRID2046480
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
The title compound was prepared from 2-acetyl-5-(2-fluoro-phenyl)-cyclohexane-1,3-dione (200 mg, 0.81 mmol), from stage 1, following the procedure describing the synthesis of 2-amino-7-(4-fluoro-phenyl)-4-methyl-7,8-dihydro-6H-quinazolin-5-one (example 3/a stage 2/3) except that the title compound was further purified by recrystallisation in methanol.
WORKUP
后处理
- customwas further purified by recrystallisation in methanol