HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Carbonate → HCID 59370512, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Carbonate | HCID 11125 | — |
| Reactant | HCID 54198127 | HCID 54198127 | — |
| Reactant | 2-Chloro-3-ethyl-4-fluorobenzonitrile | HCID 57908695 | — |
| Product | HCID 59370512 | HCID 59370512 | — |
Reaction Steps
Using 2-chloro-4-fluoro-3-ethylbenzonitrile (1.01 g), (2S,3S)-3-hydroxy-2-methylpyrrolidine (8.25 mmol) and lithium carbonate (813 mg), the title compound was obtained as a colorless solid (yield: 147 mg) by an operation similar to that in Example 3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592452B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-018b2df6d73d420ba86570856eb77747 |
| Source note | uspto-grants-2013_11 |