HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Carbonate → HCID 59370522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Carbonate | HCID 11125 | — |
| Reactant | HCID 54198127 | HCID 54198127 | — |
| Reactant | 2,3-Dichloro-4-fluoro-5-methylbenzonitrile | HCID 59370549 | — |
| Product | HCID 59370522 | HCID 59370522 | — |
Reaction Steps
Using 2,3-dichloro-4-fluoro-5-methylbenzonitrile (1.02 g), 0.9 M-dimethyl sulfoxide solution (5.56 ml) of (2S,3S)-3-hydroxy-2-methylpyrrolidine and lithium carbonate (370 mg), the title compound was obtained as a colorless solid (yield: 53 mg) by an operation similar to that in Example 3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592452B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-88363441920f4a6f878587bc186b73f1 |
| Source note | uspto-grants-2013_11 |