Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Isopropanol hydrochloride | HCID 21912024 | — |
| Reactant | HCID 86655660 | HCID 86655660 | — |
| Product | 1218764-02-3 | HCID 86655661 | 93% |
Reaction Steps
To the compound (12.4 g) obtained in step 2 was added 2N hydrogen chloride/2-propanol (100 mL), and the mixture was stirred at 50° C. for 2 hr. The reaction mixture was concentrated under reduced pressure to give the title compound (9.36 g, 93%) as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08592454B2 |
|---|
| Source dataset | uspto-grants-2013_11 |
|---|
| ORD ID | ord-00db87f2bb534e219705fd03a03b16a4 |
|---|
| Source note | uspto-grants-2013_11 |
|---|
