HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl acetonedicarboxylate → HCID 10924650, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl acetonedicarboxylate | HCID 66045 | — |
| Reactant | 2-Aminobenzonitrile | HCID 72913 | — |
| Product | HCID 10924650 | HCID 10924650 | — |
Reaction Steps
Prepared as in Example 2a from 2-aminobenzonitrile and diethyl 3-oxopentanedioate as a pale yellow solid (25%). 1H NMR (400 MHz, DMSO-d6) δ 1.19 (t, J=8.0 Hz, 3H), 1.30 (t, J=8.0 Hz, 3H), 4.08 (m, 4H), 4.28 (q, J=8.0 Hz, 2H), 7.50 (m, 1H), 7.73 (m, 2H), 8.10 (bs, 2H), 8.53 (d, J=8.0 Hz, 1H). MS 303 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592592B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-601e78c7607d42188ef1d509fb64af31 |
| Source note | uspto-grants-2013_11 |