HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Heptanol → 2-Amino-6-(heptan-4-yloxy)benzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Heptanol | HCID 11513 | — |
| Reactant | 2-Amino-6-fluorobenzonitrile | HCID 522659 | — |
| Product | 2-Amino-6-(heptan-4-yloxy)benzonitrile | HCID 66745698 | — |
Reaction Steps
Prepared as in Example 22b from heptan-4-ol and 2-amino-6-fluorobenzonitrile as a white solid (24%). 1H NMR (400 MHz, CDCl3) δ 0.92 (t, J=7.2 Hz, 6H), 1.55-1.31 (m, 8H), 3.88 (s, br, 1H), 4.33-4.27 (m, 1H), 6.26 (d, J=8.0 Hz, 1H), 6.35 (d, J=8.0 Hz, 1H), 7.20 (t, J=8.0 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592592B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-ca2f7d3fa17a48db9d67fc3a5d07b180 |
| Source note | uspto-grants-2013_11 |