HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cycloheptanol → HCID 66747005, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cycloheptanol | HCID 10399 | — |
| Reactant | 2-Amino-6-fluorobenzonitrile | HCID 522659 | — |
| Product | HCID 66747005 | HCID 66747005 | — |
Reaction Steps
Prepared as in Example 22b from cycloheptanol and 2-amino-6-fluorobenzonitrile as yellow oil (11%). 1H NMR (400 MHz, DMSO-d6) δ 1.42-1.71 (m, 10H), 1.88-1.93 (m, 2H), 4.56 (m, 1H), 5.95 (s, 2H), 6.20 (d, J=8.0 Hz, 1H), 6.30 (d, J=8.0 Hz, 1H), 7.15 (t, J=8.0 Hz, 1H). MS 231 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592592B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-872dadbc23be41a6a1a3fe45198963a6 |
| Source note | uspto-grants-2013_11 |