HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethynylcyclohexane → HCID 66746496, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethynylcyclohexane | HCID 70263 | — |
| Reactant | 2-Amino-6-bromobenzonitrile | HCID 9813038 | — |
| Product | HCID 66746496 | HCID 66746496 | — |
Reaction Steps
Prepared as in Example 21c from ethynylcyclohexane and 2-amino-6-bromobenzonitrile as a brown oil (100%). 1H NMR (400 MHz, DMSO-d6) δ 1.24-1.77 (m, 10H), 2.70 (m, 1H), 6.13 (s, 2H), 6.64 (d, J=8.0 Hz, 1H), 6.74 (d, J=8.0 Hz, 1H), 7.22 (t, J=8.0 Hz, 1H). MS 225 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592592B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-99225f0b3d264081b1d0a7cf1e27cb18 |
| Source note | uspto-grants-2013_11 |