HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine-2-carbonitrile → Picolinimidohydrazide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine-2-carbonitrile | HCID 7522 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | Picolinimidohydrazide | HCID 70493 | — |
Reaction Steps
A solution of pyridine-2-carbonitrile 20 g (192 mM), hydrazine hydrate (3 eq.) in ethanol (50 ml) is stirred at room temperature for 18 hrs. Reaction mass is then diluted with water, extracted with ethyl acetate, dried over anhydrous sodium sulphate and concentrated under vacuum to yield desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08592591B2 |
| Source dataset | uspto-grants-2013_11 |
| ORD ID | ord-4ee615420bbd4e9b98f89323a8560daa |
| Source note | uspto-grants-2013_11 |